Mild hydrothermal preparation of a layered metal hydroxide salt with microtube/rod morphology_中国颗粒学会

Mild hydrothermal preparation of a layered metal hydroxide salt with microtube/rod morphology_中国颗粒学会

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Partic. vol. 8 no. 3 pp. 192-197 (June 2010)
doi: 10.1016/j.partic.2010.03.009

Mild hydrothermal preparation of a layered metal hydroxide salt with microtube/rod morphology

He Zhang^{a, b}, Hongbin Li^a, Ying Guo^b, Guodong Li^b, Chi Fan^b, Keji Wang^b, Jiesheng Chen^a,*

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chemcj@sjtu.edu.cn

Abstract

Microtubes/rods of the layered metal hydroxide salt compound Cd₂(OH)₃(DS)·nH₂O, where DS stands for dodecyl sulfate sandwiched between two adjacent inorganic sheets, have been synthesized for the first time through a mild hydrothermal reaction route. The microtubes/rods have a diameter of about 1 μm and a length ranging from several microns to 20 μm. The growth process of microtubes/rods under the experimental conditions employed follows a dissolution–recrystallization route.

Keywords

Layered metal hydroxide salt; Cadmium hydroxide; Microtubes/rods; Hydrothermal reaction; Dodecyl sulfate; Micelle